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under high-pressure

✍ Scribed by Valim, D.; Souza Filho, A. G.; Freire, P. T. C.; Fagan, S. B.; Ayala, A. P.; Mendes Filho, J.; Almeida, A. F. L.; Fechine, P. B. A.; Sombra, A. S. B.; Staun Olsen, J.; Gerward, L.

Book ID: 118064025
Publisher: The American Physical Society
Year: 2004
Tongue: English
Weight: 57 KB
Volume: 70
Category: Article
ISSN: 1098-0121
DOI: 10.1103/physrevb.70.132103

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Cleavage of tert-butyldiphenylsilyl (TBDPS) ether was examined under high pressure conditions (1.0 GPa) using HF/pyridine in DMF. This method proved to be exceptionally suitable for deprotecting the TBDPS group that resides at the sterically hindered position. Under these conditions, various types o