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Two-Step Hantzsch Based Macrocyclization Approach for the Synthesis of Thiazole-Containing Cyclopeptides §

✍ Scribed by Nefzi, Adel; Arutyunyan, Sergey; Fenwick, Jason E.

Book ID
123610922
Publisher
American Chemical Society
Year
2010
Tongue
English
Weight
885 KB
Volume
75
Category
Article
ISSN
0022-3263

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AbstractÐ2,6-Diacetylpyridine substituted with amine or alcohol groups in the 4-position have been prepared from chelidamic acid. The key 4-chloro derivative was synthesized in high yield via a diazo intermediate and was protected as a bis-1,3-dioxane before substitution with various amino alcohol g