An NMR study of two known bis-indole alkaloids is described. In addition to conventional 1D NMR methods, 2D shift-correlated NMR experiments [ 1 Hx 1 H-COSY, 1 Hx 13 C-HMQC-1 J(C,H), 1 Hx 13 C-HMBC-n J(C,H) (n D 2 and 3)] and 2D 1 Hx 1 H-NOESY were used for 1 H and 13 C chemical shift assignments of
Two epimeric friedelane triterpenes isolated from Maytenus truncata Reiss: 1H and 13C chemical shift assignments
✍ Scribed by G. C. M. Salazar; G. D. F. Silva; L. P. Duarte; S. A. Vieira Filho; I. S. Lula
- Publisher
- John Wiley and Sons
- Year
- 2000
- Tongue
- English
- Weight
- 286 KB
- Volume
- 38
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
An NMR study of 3˛-and 3ˇ-friedelinol is described. In addition to conventional 1D NMR methods, 2D shift-correlated NMR experiments HMQC [( 1 J(C,H)], HMBC [ n J(C,H); n D 2 and 3] and 2D 1 H, 1 H-NOESY were used for 1 H and 13 C chemical shift assignments of these triterpenes.
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