✦ LIBER ✦

Two-dimensional NMR measurements of heteronuclear dipolar powder spectra using the chemical-shift-anisotropy recovery technique

✍ Scribed by Daisuke Kuwahara; Toshihito Nakai; Seiichi Miyajima

Book ID: 108312500
Publisher: Elsevier Science
Year: 1998
Tongue: English
Weight: 130 KB
Volume: 291
Category: Article
ISSN: 0009-2614
DOI: 10.1016/s0009-2614(98)00575-2

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Resolved Two-Dimensional Anisotropic-Che

Resolved Two-Dimensional Anisotropic-Chemical-Shift/Heteronuclear Dipolar Coupling Powder-Pattern Spectra by Three-Dimensional Solid-State NMR Spectroscopy

✍ A. Ramamoorthy; L.M. Gierasch; S.J. Opella 📂 Article 📅 1996 🏛 Elsevier Science 🌐 English ⚖ 104 KB

switched-angle sample spinning (SASS) (13); however, this By comparing experimental and calculated two-dimenis limited to situations where the isotropic spectra have only sional anisotropic chemical-shift/heteronuclear dipolar coua few resonances and is technically demanding because of pling [separa

A Robust Technique for Two-Dimensional S

A Robust Technique for Two-Dimensional Separation of Undistorted Chemical-Shift Anisotropy Powder Patterns in Magic-Angle-Spinning NMR

✍ S-F. Liu; J-D. Mao; K. Schmidt-Rohr 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 257 KB

A robust magic-angle-spinning experiment for separating undistorted, quasi-static chemical-shift powder patterns is presented. It is derived from the technique of R. Tycko, G. Dabbagh, and P. Mirau (1989, J. Magn. Reson. 85, 265), but uses 360 • instead of 180 • pulses. In combination with a suitabl

Direct measurement of the transverse and

Direct measurement of the transverse and longitudinal 15N chemical shift anisotropy–dipolar cross-correlation rate constants using 1H-coupled HSQC spectra

✍ Jennifer B. Hall; David Fushman 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 149 KB

## Abstract We describe direct methods for the measurement of the transverse and longitudinal ^15^N chemical shift anisotropy–dipolar cross‐correlation rates based on comparison of the ^15^N doublet components observed in ^1^H‐coupled ^1^H–^15^N HSQC‐type spectra. This allows the determination of t

Application of homonuclear and heteronuc

Application of homonuclear and heteronuclear two-dimensional chemical-shift correlation NMR spectroscopy to the complete assignment of proton and carbon-13 NMR spectra of ionophorous antibiotic X.14547 A

✍ Beloeil, J. C.; Delsuc, M. A.; Lallemand, J. Y.; Dauphin, G.; Jeminet, G. 📂 Article 📅 1984 🏛 American Chemical Society 🌐 English ⚖ 850 KB

Determination of the structure of 7-diet

Determination of the structure of 7-diethylamino-4-(1,2,3-triazol-1-yl)-2H-1-benzopyran-2-one derivatives using two-dimensional heteronuclear chemical-shift correlated NMR techniques

✍ N. N. Sveshnikov; M. A. Kirpichenok 📂 Article 📅 1994 🏛 Springer 🌐 English ⚖ 181 KB

Total assignment of the 13C-NMR spectra

Total assignment of the 13C-NMR spectra of 5H-indolo[1,7-ab][1]benzazepine and 6,7-dihydro-5H-indolo[1,7-ab][1]benzazepine using two-dimensional proton-carbon chemical shift correlation experiments

✍ Anders Hallberg; Arnold R. Martin; Gary E. Martin; Gunnar Grönberg 📂 Article 📅 1984 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 195 KB