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Tungsten(VI) and (V) complexes with some naturally occurring ligands

✍ Scribed by D.H. Brown; D. Neumann

Book ID
115973434
Publisher
Elsevier Science
Year
1975
Weight
204 KB
Volume
37
Category
Article
ISSN
0022-1902

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## Abstract Reaction of WX~6~ (X = Cl or Br) with O(SiMe~3~)~2~ in CH~2~Cl~2~, followed by addition of MeCN and a further equivalent of O(SiMe~3~)~2~ in CH~2~Cl~2~ gives [WO~2~X~2~(MeCN)~2~] in situ, which subsequently react with the dithioethers MeS(CH~2~)~2~SMe, __i__PrS(CH~2~)~2~S__i__Pr or 1,4‐