Tungsten(VI) and Molybdenum(VI) Complexe
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Martin F. Davis; William Levason; Mark E. Light; Raju Ratnani; Gillian Reid; Kee
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Article
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2007
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John Wiley and Sons
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English
β 158 KB
## Abstract Reaction of WX~6~ (X = Cl or Br) with O(SiMe~3~)~2~ in CH~2~Cl~2~, followed by addition of MeCN and a further equivalent of O(SiMe~3~)~2~ in CH~2~Cl~2~ gives [WO~2~X~2~(MeCN)~2~] in situ, which subsequently react with the dithioethers MeS(CH~2~)~2~SMe, __i__PrS(CH~2~)~2~S__i__Pr or 1,4β