Yellow crystals of the title compound, [Mn(dien) 2 ][Sb 4 S 7 ]Á-0.5H 2 O (dien = diethylenetriamine = C 4 H 13 N 3 ) were synthesized under solvothermal conditions by reacting MnSb 2 S 4 with pure dien. The Mn 2+ ion is in an octahedral environment of six N atoms of the tridentate dien molecules. T
✦ LIBER ✦
[Tris(2-aminoethyl)amine]manganese(II) heptasulfidotetraantimony(III) hemihydrate. Erratum
✍ Scribed by Schaefer, Michael ;Kurowski, Daniel ;Pfitzner, Arno ;Näther, Christian ;Bensch, Wolfgang
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 74 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê R factor = 0.030 wR factor = 0.075 Data-to-parameter ratio = 23.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.