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Triphenylphosphine-Mediated Serendipitous Synthesis of Alkyl Cinnamates Through the Reaction of 3-Hydroxy-4-Methoxybenzaldehyde and Dialkyl Acetylenedicarboxylates

✍ Scribed by Yavari, Issa; Djahaniani, Hoorieh; Moradi, Logman; Nasiri, Farough

Book ID: 111983114
Publisher: Taylor and Francis Group
Year: 2005
Tongue: English
Weight: 90 KB
Volume: 180
Category: Article
ISSN: 1042-6507
DOI: 10.1080/104265090917664

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## Abstract The reactive 1 : 1 adducts in the reaction between Ph~3~P and dialkyl acetylenedicarboxylates have been trapped with ‘tosylmethyl isocyanide’ (TsMIC; **1**) to yield dialkyl 2‐[(4‐methylphenyl)sulfonyl]‐1__H__‐pyrrole‐3,4‐dicarboxylates **3** (__Scheme 1__). The structures of the highly