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Trimethylsilyl bromide as a mild, stereoselective anomeric brominating agent

✍ Scribed by John W Gillard; Mervyn Israel

Publisher
Elsevier Science
Year
1981
Tongue
French
Weight
222 KB
Volume
22
Category
Article
ISSN
0040-4039

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Mild and practical stereoselective synth
Mild and practical stereoselective synthesis of (Z)- and (E)-allyl bromides from Baylis–Hillman adducts using Appel agents (PPh3/CBr4): a facile synthesis of semiplenamides C and E
✍ Biswanath Das; Kongara Damodar; Nisith Bhunia; Boddu Shashikanth 📂 Article 📅 2009 🏛 Elsevier Science 🌐 French ⚖ 223 KB

Appel agents (PPh 3 /CBr 4 ) have been utilized for high-yielding stereoselective synthesis of (Z)-and (E)allyl bromides from Baylis-Hillman adducts at room temperature. The method has been applied for the synthesis of naturally occurring bioactive fatty acid amides, semiplenamides C and E.

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ChemInform Abstract: Synthetic Studies on Natural Products. Part 28. Mild and Practical Stereoselective Synthesis of (Z)- and (E)-Allyl Bromides from Baylis—Hillman Adducts Using Appel Agents (PPh3/CBr4): A Facile Synthesis of Semiplenamides C (VIIIa) and E (VIIIb).
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