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Trimethylsilyl- and Trimethylstannyldimethylphosphane—Convenient and Versatile Reagents for the Synthesis of Polyfluoroaryldimethylphosphanes

✍ Scribed by Leonid I. Goryunov; Joseph Grobe; Vitalij D. Shteingarts; Bernt Krebs; Arno Lindemann; Ernst-Ulrich Würthwein; Christian Mück-Lichtenfeld

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
228 KB
Volume
6
Category
Article
ISSN
0947-6539

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Transient Silenes as Versatile Synthons – The Reaction of Dichloromethyl-tris(trimethylsilyl)silane with Organolithium Reagents
✍ Kathleen Schmohl; Thoralf Gross; Helmut Reinke; Hartmut Oehme 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 German ⚖ 108 KB

Treatment of dichloromethyl-tris(trimethylsilyl)silane (Me 3 Si) 3 Si±CHCl 2 (1), prepared by the reaction of tris(trimethylsilyl)silane with chloroform in presence of potassium tertbutoxide, with organolithium reagents (molar ratio 1 : 3) affords the bis(trimethylsilyl)methyl-disilanes Me 3 SiSiR 2