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Trifluoromethyl group disorder in crystalline 2,8-bis(trifluoromethyl)-4-hydroxymethylquinoline

✍ Scribed by Jean M. Karle; Apurba K. Bhattacharjee

Book ID
105272665
Publisher
Springer
Year
1996
Tongue
English
Weight
359 KB
Volume
26
Category
Article
ISSN
1572-8854

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A 1:1 cocrystal of 2,8-bis(trifluorometh
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✍ Sarojini, B. K. ;Narayana, B. ;Mayekar, Anil N. ;Yathirajan, H. S. ;Bolte, Micha πŸ“‚ Article πŸ“… 2007 πŸ› International Union of Crystallography 🌐 English βš– 350 KB

In the title compound, C~11~H~5~F~6~NOΒ·C~11~H~5~F~6~NO, both molecules (except F and H atoms) are essentially planar (the r.m.s. deviations for all non-H atoms are 0.008 and 0.034β€…Γ… for the alcohol and ketone, respectively). The two molecules are connected by an Oβ€”H...O hydrogen bond. The protonated