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Trichloroisocyanuric acid (TCCA) as a mild and efficient catalyst for the trimethylsilylation of alcohols and phenols with hexamethyldisilazane (HMDS) under heterogonous conditions

✍ Scribed by Ardeshir Khazaei; Mohammad Ali Zolfigol; Amin Rostami; Arash Ghorbani Choghamarani

Book ID: 119215684
Publisher: Elsevier Science
Year: 2007
Tongue: English
Weight: 129 KB
Volume: 8
Category: Article
ISSN: 1566-7367
DOI: 10.1016/j.catcom.2006.06.018

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## Abstract Structurally diverse alcohols and phenols were trimethylsilylated in a clean and efficient reaction with hexamethyldisilazane (HMDS) based on the use of I~2~ generated __in situ__ from Fe(NO~3~)~3~⋅9 H~2~O/NaI. The reaction occurs very rapid in good‐to‐high yield in CH~2~Cl~2~ at room t