Tri- and Tetrasubstituted Alkenes: Synthesis and Assignment of 3,4-Diethylhexene-2

✍ Scribed by Anny De Valck; H. J. Geise; R. A. Dommisse; Y. Luyten

• Publisher: Wiley (John Wiley & Sons)
• Year: 2010
• Weight: 192 KB
• Volume: 86
• Category: Article
• ISSN: 0037-9646
• DOI: 10.1002/bscb.19770861010

✦ Synopsis

Abstract

Dehydration of 3, 4‐diethylhexanol‐3 by means of oxalic acid yields mainly a mixture of Z and E‐isomers of 3, 4‐diethylhexene‐2. After separation by preparative GLC the identification and configurational assignment was made by ^13^C and ^1^H n.m.r.