ChemInform Abstract: New, General, and Stereoselective Synthesis of CF3-Containing Tri- and Tetrasubstituted Oxiranes and Tetrasubstituted Alkenes.
β Scribed by Masaki Shimizu; Takuya Fujimoto; Hiroshi Minezaki; Takeshi Hata; Tamejiro Hiyama
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 35 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0931-7597
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## Abstract Dehydration of 3, 4βdiethylhexanolβ3 by means of oxalic acid yields mainly a mixture of Z and Eβisomers of 3, 4βdiethylhexeneβ2. After separation by preparative GLC the identification and configurational assignment was made by ^13^C and ^1^H n.m.r.