trans-(μ-5,5′-Diethynyl-2,2′-bipyridine)bis[phenylbis(triethylphosphine)platinum(II)]
✍ Scribed by Khan, Muhammad S. ;Al-Suti, Mohammed K. ;Ahrens, Birte ;Raithby, Paul R. ;Teat, Simon J.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 312 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal synchrotron study T = 150 K Mean '(C±C) = 0.005 A Ê R factor = 0.032 wR factor = 0.068 Data-to-parameter ratio = 25.4
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.008 A Ê R factor = 0.052 wR factor = 0.118 Data-to-parameter ratio = 12.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 297 K Mean '(C±C) = 0.007 A Ê R factor = 0.047 wR factor = 0.152 Data-to-parameter ratio = 11.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title crystal structure, [Ni 2 Cl 4 {CH 2 (CH 2 CH 2 PPr i 2 ) 2 } 2 ], there are two independent molecules, one of which lies on a crystallographic inversion center. The Ni II atoms in each dinuclear molecule are in slightly distorted square-planar geometries. The two independent molecules h