trans-N,N′-Bis(3-methoxysalicylidene)cyclohexane-1,2-diamine
✍ Scribed by Aslantaş, Mehmet ;Tümer, Mehmet ;Şahin, Ertan ;Tümer, Ferhan
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 191 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 22 H 26 N 2 O 4 , was prepared by reaction of trans-1,2-cyclohexanediamine and 2-hydroxy-3-methoxybenzaldehyde. The molecular structure is stabilized by intramolecular O-HÁ Á ÁN hydrogen bonds.
📜 SIMILAR VOLUMES
Diaqua[(1R,2R)-N,N 0 0 0 -bis(3,5-dibromosalicylidene)cyclohexane-1,2-diamine-j 4 O,N,N 0 0 0 ,O 0 0 0 ]manganese(III) perchlorate dihydrate
In the title compound, [Cu(C 23 H 24 N 2 O 2 )], the Cu II atom is coordinated by two imine N and two phenol O atoms of the ligand. The geometry of the coordination is distorted tetrahedral. The dihedral angle between the N/Cu/O coordination planes is 7.37 (7) .
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.006 A Ê R factor = 0.043 wR factor = 0.100 Data-to-parameter ratio = 19.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.