trans-3-Acetyl-5-benzoyl-2-methyl-4-phenyl-4,5-dihydrofuran at 150 K
✍ Scribed by Subha Nandhini, M. ;Krishnakumar, R. V. ;Mostad, A. ;Renuga, S. ;Selvaraj, S. ;Perumal, S. ;Natarajan, S.
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 298 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 29 H 27 NO 7 , has a non-planar con®guration. The methoxycarbonylmethyl group exhibits an E con®guration. The crystal structure is stabilized by intermolecular OÐHÁ Á ÁO and CÐHÁ Á ÁO contacts.
The title compound, C~26~H~26~N~2~O~7~, is a thiamidine derivative. Geometric parameters are in the usual ranges. The crystal packing is stabilized by a classical N—H...O hydrogen bond, several weak C—H...O hydrogen bonds and a π–π stacking interaction.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.140 Data-to-parameter ratio = 13.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.