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Towards the rehabilitation of the Leuckart reductive amination reaction using microwave technology

✍ Scribed by André Loupy; Daphné Monteux; Alain Petit; Jesús Ma Aizpurua; Esther Domínguez; Claudio Palomo

Book ID
103407931
Publisher
Elsevier Science
Year
1996
Tongue
French
Weight
176 KB
Volume
37
Category
Article
ISSN
0040-4039

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The Mathews' reaction is a one-pot preparation of carboxylic acids from their corresponding nitriles or amides by a 'dry' hydrolysis with phthalic acid or anhydride in the absence of water and solvent. Excellent isolated yields and selectivity (up to 99%) were attained within short reaction times (t