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Total synthesis of the monoterpenoidalkaloid (±)-tangutorine

✍ Scribed by van den Broek, Sebastiaan (Bas) A. M. W. ;Lemmers, Jaap G. H. ;van Delft, Floris L. ;Rutjes, Floris P. J. T.

Book ID
120165852
Publisher
Royal Society of Chemistry
Year
2012
Tongue
English
Weight
303 KB
Volume
10
Category
Article
ISSN
1477-0520

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ChemInform Abstract: First Total Synthes
ChemInform Abstract: First Total Synthesis of (.+-.)-Tangutorine.
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Synthesis of Tangutorine.
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Synthesis of Tangutorine
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✍ Tse-Lok Ho; Chun-Kuei Chen 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 German ⚖ 71 KB

Tangutorine (1) in the racemic form has been assembled from tryptamine and aldehyde 3. The synthetic design was based on uncovering a hidden symmetry in the nontryptamine portion of the norketone 2. A five-step process with an overall yield of 7% was developed in which 2 was transformed into the tar