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Total synthesis of arenamide A and its diastereomer

✍ Scribed by S. Chandrasekhar; G. Pavankumarreddy; K. Sathish

Book ID
104096997
Publisher
Elsevier Science
Year
2009
Tongue
French
Weight
386 KB
Volume
50
Category
Article
ISSN
0040-4039

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✦ Synopsis

Arenamide A and its diastereomer have been synthesized in a convergent fashion. The key steps involved in this synthesis are Sharpless asymmetric epoxidation, C-C bond formation, and macrolactamization.

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## Abstract The first synthesis of racemic silyhermin (__rac__‐1a) and its 2‐diastereomers 1b (as a ca. 1:1 mixture) was accomplished by starting from caffeic acid ethyl ester and coniferyl alcohol.