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Total synthesis of anthrasteroids—III : The preparation of some 3-phenyl-2,4-diaza-anthraestranes

✍ Scribed by K. Wiedhaup; H.O. Huisman

Book ID: 103397421
Publisher: Elsevier Science
Year: 1968
Tongue: French
Weight: 611 KB
Volume: 24
Category: Article
ISSN: 0040-4020
DOI: 10.1016/0040-4020(68)88028-7

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## Abstract 1,2,3,4‐Tetrahydrodibenzofuran‐1‐ones were obtained by __Michael__ addition of 1,3‐cyclohexadione (**2**) to __o__‐benzoquinone (**3**) and to __p__‐benzoquinones **8** and **11** (__Scheme 2__). In addition to the expected 7,8‐disubstituted adduct **14**, the ZnCl~2~‐catalyzed reaction