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Total assignment of the 1H NMR spectra of 5H-indolo[1,7-ab] [1]benzazepine,6,7-dihydro-5H-indolo[1,7-ab][1]benzazepine and pyrrolo[3,2,1-kl ] phenothiazine

✍ Scribed by Anders Hallberg; Torsten Dahlgren; Arnold Martin; Kenner Christiansen

Book ID: 112126977
Publisher: Journal of Heterocyclic Chemistry
Year: 1983
Tongue: English
Weight: 219 KB
Volume: 20
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570200109

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## Synthesis of 7,12-Dihydro-indo~o[3~[l]benzazepin-6-(~~nes and gll-Dihydr~.thieno-[3'3':~]~zepino[qS-b]indol-5(4H)-one The title compounds 4 and 6 were prepared by Fischer indole synthesis. 4a is substituted in 10-position by reaction with bromine in glacial acetic acid. A fast ring inversion is