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Total Assignment of 1H and 13C NMR Chemical Shifts of a Natural Anthocyanidin, Apigeninidin, Using Two-Dimensional COLOC and HMBC Techniques

✍ Scribed by Marie Kouda-Bonafos; Mouhoussine Nacro; Bernard Ancian

Publisher: John Wiley and Sons
Year: 1996
Tongue: English
Weight: 210 KB
Volume: 34
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199605)34:5<389::aid-omr888>3.0.co;2-9

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✦ Synopsis

The 'H and "C NMR spectra of apigeninidin chloride were assigned utilizing the two-dimensional 6,, S, correlation and COLOC and HBMC techniques. The full 13C NMR data are reported for the first time. A good correlation was found between 13C chemical shifts and carbon charge obtained by AM1 calculation.

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