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Total Assignment of the 1H and 13C NMR Chemical Shifts of Three Bisabolane Hydrocarbons by 2D-NMR Spectroscopy

✍ Scribed by Lai-King Sy; Geoffrey D. Brown

Publisher: John Wiley and Sons
Year: 1997
Tongue: English
Weight: 151 KB
Volume: 35
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199706)35:6<424::aid-omr84>3.0.co;2-c

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✦ Synopsis

Three known bisabolane hydrocarbons, a-trans -bergamotene, sesquiphellandrene and zingiberene, were isolated from the aerial parts of Alpinia densibracteata . Their 1H and 13C NMR spectra were completely assigned by using a combination of 13C DEPT and 2D-NMR experiments (1H-1H COSY, single-bond 13C-1H correlation, long-range 13C-1H correlation and INADEQUATE).

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