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Thyroxine analogues: synthesis of 3,3?,5,5?-tetramethyl-L-thyronine

✍ Scribed by Block, Paul; Coy, David H.

Book ID
118276944
Publisher
Royal Society of Chemistry
Year
1972
Weight
280 KB
Volume
0
Category
Article
ISSN
1472-7781

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Dl-3.5.3′.5′-Tetramethyl-Thyronin
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## Abstract dl‐3.5.3′.5′‐Tetramethyl‐thyronin (II) wird, ausgehend von 2.6‐Dimethylanilin, in 10 Stufen mit einer Gesamtausbeute von 5% d. Th. dargestellt. Seine Eigenschaften werden mit denen von dl‐Thyronin, dl‐Thyroxin, dl‐3.5.3′.5′‐Tetranitro‐thyronin und entsprechend substituierten Thio‐thyron

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Absa'aet" The moao-and di-iodo derivatives of l-oxaspiro[2,5]bieyclooeta-4,7-dien-6-one, 8 and 9, reacted readily with 3,5-diiodo-L-t3,rosine at pH 8.0 to give 3,5,3'-triiodo-L-thyronine (1"3) and thyroxine in 70% and 94% yields respectively. In turn, 8 and 9 were prepared by the sodium bismuthate o

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