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Three-component reaction between elemental sulfur, primary phosphines, and amines: straightforward synthesis of organylammonium trithiophosphonates

✍ Scribed by Artem'ev, Alexander V.; Malysheva, Svetlana F.; Belogorlova, Nataliya A.; Gusarova, Nina K.

Book ID
120331809
Publisher
Taylor and Francis Group
Year
2013
Tongue
English
Weight
235 KB
Volume
34
Category
Article
ISSN
1741-5993

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πŸ“œ SIMILAR VOLUMES

Reaction of primary phosphines with elem
Reaction of primary phosphines with elemental sulfur and alkali metal hydroxides (MOH, M = Na, K, Cs): a novel and facile three-component synthesis of trithiophosphonates
✍ Alexander V. Artem’ev; Nina K. Gusarova; Svetlana F. Malysheva; Victor I. Mamaty πŸ“‚ Article πŸ“… 2011 πŸ› Elsevier Science 🌐 French βš– 338 KB

Primary phosphines readily react with elemental sulfur and alkali metal hydroxides (MOH, M = Na, K, Cs) in the molar ratio 1:3:2 under mild conditions (70 Β°C, 0.5 h, ethanol) to afford alkali metal trithiophosphonates in good to high yields (72-90%).