Thin-layer electrophoresis of indole derivatives
โ Scribed by Bhavdish N. Johri
- Book ID
- 104145245
- Publisher
- Elsevier Science
- Year
- 1970
- Tongue
- English
- Weight
- 421 KB
- Volume
- 50
- Category
- Article
- ISSN
- 1873-3778
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โฆ Synopsis
Thin-layer electrophoresis of indole derivatives NOTES TABLE I ELECTROPHORETIC MOBILITES OF INDOLES AT DtFFERENT VOLTAGESa A: acetate buffer, pH 5.2; current, I IO V; time, 5 11. B: pyriclinc-acetic acid, pH 6. I ; current, 440 V; time, 1.5 h. C: acetate buffer, pH 6.0; current, 220 V; time, 3 h. D: acetate buffer, pH 6.2; current, 220 V; time, 3 h. E: pyridine-acetic acid, pH 6.1; current, 220 V; time, 3 h. F: borate buffer, pH 10.0; current, 220 V; time, 3 h. Indoles Electrophovetic systems A B c D E I; IAA +0.10 3-0.10 fo.07 fo.07 +o.15 fo.08 IAN -0.05 -0.04 -0.05 -0.05 -0.03 -0.12 IBA -t-o.06 -t_ 0.05 fo.03 +o*o4 -to.12 +o.o4 TP -0.05 -0.01 -0.07 -0.07 -0.05 -0.11 T -0.24 -0.20 -0.20 -0.23 -0.19 -0.21 5-HT -0.29 -0.17 -0.23 -0.25 .-0.20 -0.24 5-HTP -0.02 -0.08 -0.07 -0.07 -0.12 a The electrophorctic mobility is expressed in arbitrary units; for details see text.
๐ SIMILAR VOLUMES
A sensitive ptlrt~f~~rmafdeh~de spray reagent for the thin-layer chromato~raphic detection of indofe derivatives at the nanogram level is described\_ Paraformafdehyde is dissolved in sfightl\_v alkaline etfmnof and the ethnnofic solution is neutralized by addition of acetic acid. The tluorescence is