Thin layer chromatography of dansyl amino acid derivatives
✍ Scribed by Zdeněk Deyl; Jan Rosmus
- Publisher
- Elsevier Science
- Year
- 1965
- Tongue
- English
- Weight
- 549 KB
- Volume
- 20
- Category
- Article
- ISSN
- 1873-3778
No coin nor oath required. For personal study only.
✦ Synopsis
The Eastman Chromatogram sheets Type 1<301R wcrc used as well as Silicagcl layers. The Rp vducs are unchrtngccl.
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Amino acid hydaneoins were detected directly in amounts of 0.2-O.Spg with tevt.-bueyl hypochlorite. The amino acid hydantoins' were separated by thin-layer chromatography using the following solve@ systems: (I) chloroform-ethanol-formic acid (2: 1: 1); (II) rz-but.yl acetate-ethanol-formic acid (12
A simple, rapid, and reliable technique for identifying small amounts of phenylthiohydantoin (PTH) derivatives has been developed for use in the analysis by Edman degradation of small amounts of peptides isolated from fingerprints (10). Solvent systems used in paper and column chromatography of PTH