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Thermogravimetric study of the intercalation of acetic acid and of water by Al3+-exchanged montmorillonite

✍ Scribed by A.A. Al-Owais; James A. Ballantine; J.Howard Purnell; John.M. Thomas


Book ID
103692455
Publisher
Elsevier Science
Year
1986
Weight
741 KB
Volume
35
Category
Article
ISSN
0304-5102

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## Abstract ^17^O‐enriched acetic acid (2.5% in ^17^O) was synthesized by hydrolysis of acetic anhydride with ^17^O‐enriched water. The reaction was monitored by ^17^O and ^1^H NMR spectroscopy. Acetic anhydride, ^17^O‐enriched in both the ether and the carbonyl oxygens, was observed as an intermed