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Thermal rearrangement of 6,6-dichloro-3,3-dimethyl-2-oxabicyclo[3.1.0]hexane. Novel case of steric hindrance to ionization

โœ Scribed by De Selms, Roy C.; Kreibich, Ursula T.

Book ID
126234588
Publisher
American Chemical Society
Year
1969
Tongue
English
Weight
353 KB
Volume
91
Category
Article
ISSN
0002-7863

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## Novel Conversion of Perfluoro(2,6-dimethyl-1-azacyclohexene) to 3,3,4,4,5-Pentafluoro-2,6-diphenyl-2,6-bis (trifluoromethyl)-1azabicyclo[3.1.0]hexane. -Treatment of perfluoro-azacyclohexene (I) with 2 equiv. of phenyllithium (V) in a cyclohexane/Et 2 O mixture provides access to azabicyclohex