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Thermal decomposition of potassium, rubidium, and cesium ozonides

✍ Scribed by A. B. Tsentsiper; M. S. Dobrolyubova

Book ID
112421493
Publisher
Springer
Year
1972
Tongue
English
Weight
277 KB
Volume
21
Category
Article
ISSN
1573-9171

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v(NOj).-MS (CI), Varian MAT 312: MH' (m/z 570).-4b and 4c were prepared analogously. 4b : dark-red crystals, m.p. 8 8 T , yield 25.5%-C=P), 207.3 (d, 'J(PC)=19.7 Hz, C=O), 1.7 (s, (CH3),Si0).-4c: darkred crystals, m.p. 9 9 T , yield 37'Yo.-''P-NMR: 6= 194.4 (s).-I3C-C=O), 0.40 (s, (CH3)3SiO). [8] St

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In a recent report on the photochemistry of ozonides we found the major products to consist of hydrocarbons which were, in part, formed by way of radical cage recombinations. (II The present study is concerned with the thermal decomposition of the same ozonides and has yielded mechanistic informatio