✦ LIBER ✦

Crystal Structures of Potassium Ozonide and Rubidium Ozonide

✍ Scribed by Dipl.-Chem. Wolfgang Schnick; Prof. Dr. Martin Jansen

Publisher: John Wiley and Sons
Year: 1985
Tongue: English
Weight: 234 KB
Volume: 24
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.198500541

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✦ Synopsis

v(NOj).-MS (CI), Varian MAT 312: MH' (m/z 570).-4b and 4c were prepared analogously. 4b : dark-red crystals, m.p. 8 8 T , yield 25.5%-C=P), 207.3 (d, 'J(PC)=19.7 Hz, C=O), 1.7 (s, (CH3),Si0).-4c: darkred crystals, m.p. 9 9 T , yield 37'Yo.-''P-NMR: 6= 194.4 (s).-I3C-C=O), 0.40 (s, (CH3)3SiO). [8] Stable phosphinocarbonyl complexes of the type (C,(CH,),)(CO),M-C(O)P(tBu)(sijcH,),) of iron (6"P=75.1 (C,D,

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