## Abstract Preparative resolution of the enantiomers of several chiral dihydrofuranones, known to be important flavor compounds, has been achieved by combining the use of bonded Ξ²βcycloβdextrin as chiral stationary phase with closedβloop recycling chromatography. The purity of the separated enanti
β¦ LIBER β¦
Theoretical study of recycling in preparative chromatography
β Scribed by Andreas Seidel-Morgenstern; Georges Guiochon
- Publisher
- American Institute of Chemical Engineers
- Year
- 1993
- Tongue
- English
- Weight
- 952 KB
- Volume
- 39
- Category
- Article
- ISSN
- 0001-1541
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Conformational features of a chiral stationary phase used in column chromatography are discussed. The syn forms invoked in chiral recognition models are consistent with MNDO and MM2 calculations. It is speculated that the inherent flexibility of the syn form makes these phases effective templates fo