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The use of DSS as an internal standard in PMR studies of nucleic acid interactions

✍ Scribed by David. H. Live; Sunney I. Chan

Publisher: John Wiley and Sons
Year: 1973
Tongue: English
Weight: 176 KB
Volume: 5
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1270050606

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

Two commonly used PMR internal reference compounds, 3‐(trimethyl silyl) propane sulfonic acid sodium salt (DSS) and 3‐(trimethyl silyl) sodium propionate (TSP), have been shown to interact with purine in aqueous solution, causing significant shifts in the resonance position of their reference protons. Tetramethyl ammonium chloride (TMACl) appears to be a more suitable reference compound for such studies.

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