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The use of a high resolution NMR spectrometer for recording solid state 31P spectra

โœ Scribed by K.B. Dillon; T.C. Waddington

Book ID
113372640
Publisher
Elsevier Science
Year
1971
Tongue
English
Weight
496 KB
Volume
27
Category
Article
ISSN
1386-1425

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An AB3 high-resolution NMR spectrum in t
An AB3 high-resolution NMR spectrum in the solid state: 31P in P4S3
โœ E.R. Andrew; W.S. Hinshaw; A. Jasinski ๐Ÿ“‚ Article ๐Ÿ“… 1974 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 206 KB

A hi&resolution 31P NMR spectrum has been recorded in polycrystalline tetraphosphoros trisulphide PqSa\_ The spectrum exhibits the resolved doublet and quartet structure characteristic of an AB3 type spectrum, with chemical shift difference 185 f 2 ppm and J = 70 + 3 Hz.