High-resolution solid-state magic angle spinning (73)Ge NMR spectra of some organogermanium compounds were measured. Most tetrasubstituted germanes with identical substituents exhibited signals except for one case. Tetrasubstituted germanes with two kinds of different but somewhat similar substituen
β¦ LIBER β¦
High resolution solid state MAS 31P NMR spectra of phosphinated montmorillonite catalysts
β Scribed by K.Ravi Kumar; B.M. Choudary; Boris Moroz; V.M. Mastikhin; V.A. Likholobov
- Book ID
- 103692590
- Publisher
- Elsevier Science
- Year
- 1987
- Weight
- 327 KB
- Volume
- 40
- Category
- Article
- ISSN
- 0304-5102
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27Al decoupling has been used to remove residual J-coupling interactions between 31P and 27Al in microporous aluminophosphates AlPO4-14 and AlPO4-40. In combination with 1H high-power decoupling, 27Al adapted decoupling yields 31P spectra with optimal sensitivity and resolution. The importance of do