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The use of 17O-NMR in the study of bond cleavage during the hydrolysis of sulphate esters

✍ Scribed by Anthony Marker; A.B. Roy

Book ID
113264308
Publisher
Elsevier Science
Year
1983
Tongue
English
Weight
410 KB
Volume
742
Category
Article
ISSN
0167-4838

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## Abstract ^17^O‐enriched acetic acid (2.5% in ^17^O) was synthesized by hydrolysis of acetic anhydride with ^17^O‐enriched water. The reaction was monitored by ^17^O and ^1^H NMR spectroscopy. Acetic anhydride, ^17^O‐enriched in both the ether and the carbonyl oxygens, was observed as an intermed