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The use of 13CH satellite NMR spectra in structure determination: (Chlorovinyl) dichlorophosphine

✍ Scribed by M. Lana Sheer

Publisher
John Wiley and Sons
Year
1974
Tongue
English
Weight
191 KB
Volume
6
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

^13^CH satellite NMR spectra have been employed in the analysis of an unknown reaction product. Observation of the deceptively simple ^1^H NMR spectrum did not, in this instance, yield sufficient information for identification of the compound. However, with the aid of the satellite parameters the reaction site became clearly defined and the structure was assigned as α‐(chlorovinyl)‐dichlorophosphine. These unique spectral parameters are discussed and compared to those of similar ethylenic species.

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