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The Tethered Aminohydroxylation (TA) Reaction

✍ Scribed by Timothy J. Donohoe; Peter D. Johnson; Richard J. Pye

Publisher: John Wiley and Sons
Year: 2003
Weight: 51 KB
Volume: 34
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200339248

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A concise stereoselective route to the dysiherbaine tetrahydropyran core was achieved in 9 steps and 39% overall yield. Donohoe's improved tethered aminohydroxylation conditions were employed to concurrently install the amino and alcohol groups and construct the tetrahydropyran ring, which features