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The synthesis ofN-ethyl-n-butylamine by amines disproportionation

✍ Scribed by Lu-feng Xu, Jia-min Huang, Chao Qian, Xin-zhi Chen…

Book ID
120765744
Publisher
Springer Netherlands
Year
2012
Tongue
English
Weight
388 KB
Volume
39
Category
Article
ISSN
0922-6168

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Ethyl chlorocarbonate-14C and its applic
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✍ F. J. Marshall; R. E. McMahon 📂 Article 📅 1970 🏛 John Wiley and Sons 🌐 French ⚖ 262 KB

## Abstract A convenient method for the preparation of ethyl chlorocarbonate‐^14^C is described. This has led to a facile synthesis of N‐methyl‐^14^C secondary amines by lithium aluminum hydride reduction of an intermediate ^14^C‐carbamate. The reaction has also been employed in the preparation of