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The Synthesis of N-(2-Benzyl-4-Δ 2 -oxazolinoyl)-valine 1

✍ Scribed by Adkins, Homer; Ross, Robert M.; Schroeder, Dorothy Chynoweth; Mahoney, C. Lynn; Gilbert, Walter W.

Book ID
126480991
Publisher
American Chemical Society
Year
1954
Tongue
English
Weight
820 KB
Volume
76
Category
Article
ISSN
0002-7863

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Addition of various amines to the 3,3-bis(trifluoromethyl)acrylamides 10a and 10b gave the tripeptides 11a -11f, mostly as mixtures of epimers (Scheme 3). The crystalline tripeptide 11f 2 was found to be the N-terminal (2-hydroxyethoxy)-substituted (R,S,S)-ester HOCH 2 CH 2 O-d-Val(F 6 )-MeLeu-Ala-O