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Improved synthesis of N-benzyl-5-ethyl-1,2,3,4-tetrahydropyridine

✍ Scribed by Norman, Mark H.; Heathcock, Clayton H.

Book ID: 120290004
Publisher: American Chemical Society
Year: 1988
Tongue: English
Weight: 303 KB
Volume: 53
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00249a050

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## Abstract Fourteen novel __N__‐(substituted phenylcarbonylamino)‐4‐ethyl‐1,2,3,6‐tetrahydropyridines **9** were synthesized in fair to good yields. 4‐Ethylpyridine **5** reacted with __O__‐mesitylenesulfonylhydroxylamine (__O__‐MSH) **4** to furnish __N__‐amino‐4‐ethylpyridinium mesitylenesulfona