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The synthesis of a cyclophane containing two bridged annulene units

✍ Scribed by Reginald H Mitchell; Xin Jin

Book ID
103411008
Publisher
Elsevier Science
Year
1995
Tongue
French
Weight
211 KB
Volume
36
Category
Article
ISSN
0040-4039

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Dehydrobenzoannulene derivatives 5-7 containing isolated alkene linkages were synthesized by combining an in-situ Pd/Cu-mediated cross-coupling with an intramolecular cyclization strategy. 1 H NMR studies of these macrocycles and comparison with related systems verify that highly alkynyl-