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ChemInform Abstract: Synthesis and Spectroscopic Studies of Expanded Planar Dehydrotribenzo[n]annulenes Containing One or Two Isolated Alkene Units.

✍ Scribed by W. Brad Wan; Ryan C. Chiechi; Timothy J. R. Weakley; Michael M. Haley

Publisher
John Wiley and Sons
Year
2010
Weight
35 KB
Volume
33
Category
Article
ISSN
0931-7597

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Synthesis and Spectroscopic Studies of E
Synthesis and Spectroscopic Studies of Expanded Planar Dehydrotribenzo[n]annulenes Containing One or Two Isolated Alkene Units
✍ W. Brad Wan; Ryan C. Chiechi; Timothy J. R. Weakley; Michael M. Haley 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 English ⚖ 357 KB 👁 1 views

Dehydrobenzoannulene derivatives 5-7 containing isolated alkene linkages were synthesized by combining an in-situ Pd/Cu-mediated cross-coupling with an intramolecular cyclization strategy. 1 H NMR studies of these macrocycles and comparison with related systems verify that highly alkynyl-