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The synthesis of 5β,7β(H),10α-eudesm-4(14)en-1-one. Comments on the structure of canarone.

✍ Scribed by L.H. Zalkow; S.J. Steindel; N.G. Schnautz; C.K. Kellog

Book ID
104238244
Publisher
Elsevier Science
Year
1973
Tongue
French
Weight
195 KB
Volume
14
Category
Article
ISSN
0040-4039

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✍ Edward J. Parish; George J. Schroepfer Jr. 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 301 KB

## Abstract Oxidation of 5α‐cholest‐8(14)‐ene‐3β,7α,15α‐triol with silver carbonate‐celite gave 5α‐cholest‐8(14)‐ene‐7α,15α‐diol‐3‐one in 88% yield. Treatment of the latter compound with tritiated water under basic conditions gave a labeled product which was reduced with lithium tri‐__tert__‐butoxy