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Biosynthesis of 4-14C- and 7α-3H-labeled 20α-hydroxypregn-4-en-3-one and 7α-3h-3β, 20α-dihydroxypregn-5-ene

✍ Scribed by Robert H. Purdy; Märta Halla; Brian Little

Book ID
118977036
Publisher
Elsevier Science
Year
1964
Tongue
English
Weight
547 KB
Volume
4
Category
Article
ISSN
0039-128X

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Inhibitors of sterol synthesis. Synthesis of [2,4-3H]5α-cholest-8(14)-ene-3β,7α,15α-triol and [2,4-3H]5α-cholest-8(14)-en-38-ol-15-one
✍ Edward J. Parish; George J. Schroepfer Jr. 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 301 KB

## Abstract Oxidation of 5α‐cholest‐8(14)‐ene‐3β,7α,15α‐triol with silver carbonate‐celite gave 5α‐cholest‐8(14)‐ene‐7α,15α‐diol‐3‐one in 88% yield. Treatment of the latter compound with tritiated water under basic conditions gave a labeled product which was reduced with lithium tri‐__tert__‐butoxy