The synthesis of [18F]Xenon difluoride from [18F]fluoride gas
✍ Scribed by Raman Chirakal; Gunter Firnau; Gary J. Schrobilgen; John Mckay; E.S. Garnett
- Book ID
- 107769281
- Publisher
- Elsevier Science
- Year
- 1984
- Weight
- 420 KB
- Volume
- 35
- Category
- Article
- ISSN
- 0020-708X
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📜 SIMILAR VOLUMES
Electrophilic radiofluorination reagents with greatly improved specific activity (102-103-fold) were successfully used to radiolabel the chemically labile ligand 2-oxoquazepam. [ISF]Fluorine was synthesized in an electrical discharge chamber by exchanging varying amounts of carrier fluorine with hig
## Abstract A rapid synthesis of 2‐deoxy‐2‐fluoro‐D‐glucose **(3)** from xenon difluoride is described. Reaction of 3,4,6‐tri‐O‐acetyl‐D‐glucal **(1)** with xenon difluoride in ethyl ether in the presence of BF~3~·OEt~2~ for 20 minutes gave 2‐deoxy‐2‐fluoro‐ 3,4,6‐tri‐O‐acetyl‐D‐glucopyranosyl fluo