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The Synthesis and Optical Resolution of 4,5,8-Trimethyl-1-phenanthrylacetic Acid 1

✍ Scribed by Newman, Melvin S.; Hussey, Allen S.

Book ID: 126418336
Publisher: American Chemical Society
Year: 1947
Tongue: English
Weight: 563 KB
Volume: 69
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01204a026

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## Abstract The synthesis of specifically labeled 2,5,8‐trimethyl‐3,4‐dihydro‐1(2H)‐naphthalenone‐2‐d and 3,5,8‐trimethyl‐3,4‐dihydro‐1(2H)‐naphthalenone‐2,2‐d~2~ through α‐proton exchange using neat trifluoroacetic acid‐d is described.