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The syntheses and crystal structures of two incomplete cubane-like mixed-metal clusters: [{WAg2S3C5H5NS}(PPh3)2(X)] · CH2Cl2(X= S, O)

✍ Scribed by Quanming Wang; Xintao Wu; Qun Huang; Tianlu Sheng

Publisher
Springer
Year
1996
Tongue
English
Weight
631 KB
Volume
7
Category
Article
ISSN
1040-7278

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Two new 1,2,3,5-dithiadiazoles, [4-(4Ј-C 5 H 4 N)CN 2 S 2 ] (L 1 ) and [4-(3Ј-C 5 H 4 N)CN 2 S 2 ] (L 2 ), with different pyridyl groups at the 4-position were prepared. As Lewis bases, the dithiadiazoles reacted with Lewis acids via their pyridyl groups to form acid-base adducts with retention of t