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The Structure of Two Anhydrous Polymorphs of Caffeine from Single-Crystal Diffraction and Ultrahigh-Field Solid-State 13 C NMR Spectroscopy

✍ Scribed by Enright, Gary D.; Terskikh, Victor V.; Brouwer, Darren H.; Ripmeester, John A.

Book ID: 125547295
Publisher: American Chemical Society
Year: 2007
Tongue: English
Weight: 650 KB
Volume: 7
Category: Article
ISSN: 1528-7483
DOI: 10.1021/cg070291o

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## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should